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International Journal of Phytomedicine and Phytotherapy

Table 5 Spectral data of n-hexane soluble fraction of Sargassum ilicifolium

From: Hepatoprotective activity against acetaminophen-induced liver dysfunction and GC-MS profiling of a brown algae Sargassum ilicifolium

Peak # Systemic name Molecular formula Mol. wt. tR (min) Conc. Characteristic mass fragments,
m/z (rel.% BP)
Area
Sum (%)
1. Methyl 3,3-dichloropropenoate C4H4Cl2O2 154 6.104 0.092 123(99), 125(66), 60(20), 63(15), 127(14), 95(13), 154(99), 97(92), 156(77), 62(76) 0.092
2. Benzaldehyde C7H6O 106 8.132 0.092 106(99), 105(94), 77(92), 51(36), 50(18), 78(16), 52(98), 107(77), 74(63), 39(60) 0.092
3. 3, 3, 5, 5-Tetramethylcyclohexanol C10H20O 156 10.201 0.16 123(99), 41(44), 57(42), 81(29), 55(28), 56(26), 85(25), 29(20), 43(19), 39(18) 0.16
4. Benzyl Alcohol C7H8O 108 11.457 0.242 79(99), 108(89), 107(69), 77(54), 51(22), 91(18), 78(11), 50(10), 39(10), 80(95) 0.242
5. 1-Propene, 2, 3-dibromo- C3H4Br2 198 12.987 0.107 119(99), 121(98), 39(90), 200(71), 198(37), 202(35), 40(30), 38(21), 37(13), 93(98) 0.107
6. l-(+)-Ascorbic acid 2,6-dihexadecanoate C38H68O8 652 14.737 0.071 57(99), 73(91), 43(84), 60(74), 71(63), 55(57), 69(44), 41(43), 129(43), 85(41) 0.071
7. 2-Oxepanone C6H10O2 114 15.122 0.109 42(99), 55(96), 41(49), 84(44), 56(30), 28(26), 27(22), 70(21), 39(20), 114 (20) 0.109
8. Palmitic anhydride C32H62O3 494 15.612 0.1 98(99), 256(37), 55(36), 43(27), 57(27), 83(26), 73(25), 112(24), 84(23), 239(23) 0.1
9. Cyclopropane, 1, 1-dichloro-2-methyl-3-pentyl- C9H16Cl2 194 16.419 0.086 110(99), 41(97), 43(96), 39(77), 56(74), 112(65), 55(60), 42(48), 69(36), 65(30) 0.086
10. Cyclopropane, 1,1-dichloro-2,2-dimethyl- C5H8Cl2 138 18.954 0.089 103(99), 123(96), 41(63), 125(61), 87(59), 67(43), 39(34), 105(33), 42(25), 89(24) 0.089
11. 2-Hexanone, 6-(acetyloxy) C8H14O3 158 19.297 0.14 43(99), 98(17), 56(10), 55(70), 41(60), 101(60), 58(50), 61(50), 83(50), 42(30) 0.14
12. Bis-(2,2,6,6-tetramethyl,-4-piperidyl) amide oxalic acid C20H38N4O2 366 20.732 0.149 124(99), 98(66), 77(56), 105(56), 58(44), 42(39), 122(31), 41(21), 51(21), 141(17) 0.149
13. 2-Decenal, (E)- C10H18O 154 22.112 0.104 41(99), 43(99), 55(71), 70(55), 29(53), 39(48), 27(45), 57(43), 83(34), 69(30) 0.104
14. Benzeneacetic acid, 4-tetradecyl ester C22H36O2 332 24.939 0.116 91(99), 57(59), 43(42), 41(37), 71(33), 55(30), 39(21), 85(20), 44(19), 196(17) 0.116
15. 5,5,10,10-Tetrachlorotricyclo[7.1.0.0(4,6)]decane C10H12Cl4 272 25.683 0.066 109(99), 91(90), 111(73), 65(67), 39(65), 77(61), 127(53), 51(46), 79(38), 101(36) 0.066
16. 4-(3-Hydroxy-2,2,6-trimethyl-7-oxa-bicyclo[4.1.0]hept-1-yl)-but-3-en-2-one C13H20O3 224 26.612 0.187 43(99), 123(97), 109(50), 41(19), 55(18), 124(17), 165(16), 101(14), 125(12), 83(11) 0.187
17. 1-Nonene, 2-ethyl-3-(methoxymethoxy) C13H26O2 214 29.205 0.075 45(99), 129(36), 83(15),55(10), 41(73), 97(64), 69(63), 43(55), 70(49), 99(49) 0.075
18. 2-(2-Chloromethylene-1-hydroxycyclohexyl) propionic acid, methyl ester C11H17ClO3 232 29.628 0.085 145(99), 109(75), 81(45), 88(44), 57(35), 147(35), 197(32), 79(19), 41(19), 91(19) 0.085
19. 1-Ethyl-1-(undec-10-enyloxy)-1-silacyclohexane C18H36OSi 296 30.614 0.072 115(99), 41(85), 55(61), 45(54), 29(43), 87(41), 43(39), 27(33), 39(27), 267(26) 0.072
20. 1-Methyl-1-(2-tridecyl)oxy-1-silacyclopentane C18H38OSi 298 30.911 0.131 143(99), 41(73), 43(69), 39(42), 55(39), 99(36), 45(27), 57(25), 42(21), 69(17) 0.131
21. 1-Pentene, 1,1,5-trichloro- C5H7Cl3 172 31.971 0.068 65(99), 101(90), 136(47), 109(46), 138(31), 111(30), 39(29), 103(28), 73(18), 96(15) 0.068
22. 2-Oxa-7-thiatricyclo[4.4.0.0(3,8)]decan-4-ol, 4-methylbenzenesulfonate, stereoisomer (1-α, 3-α, 4-β, 6-α, 8-α)- C15H18O4S2 326 33.222 0.074 91(99), 97(83), 154(68), 113(55), 41(55), 81(52), 65(46), 326(46), 119(38), 45(36) 0.074
23. Octahydrobenzo[b]pyran, 4a-acetoxy-5,5,8a-trimethyl- C14H24O3 240 33.496 0.077 111(99), 124(85), 43(69), 69(49), 41(45), 180(44), 55(28), 97(23), 71(22), 96(22) 0.077
24. 1-Octyne, 3-(methoxymethoxy)- C10H18O2 170 33.78 0.086 45(99), 26(71), 99(56), 84(15), 41(14), 67(10), 56(99), 55(97), 39(884), 43(82) 0.086
25. Spiro(1,3-dioxolane)-2,3′-(5′-androsten-16′-ol) C21H32O3 332 33.974 0.091 99(99), 55(13), 100(10), 91(88), 79(59), 105(56), 41(51), 77(46), 86(43), 332(41) 0.091
26. Oleic Acid C18H34O2 282 35.904 0.146 55(99), 41(60), 69(56), 57(47), 43(35), 73(32), 83(32), 29(25), 56(22), 60(19) 0.146
27. Hexanoic acid, 2-ethyl-, oxybis (2,1-ethanediyloxy-2,1-ethanediyl) ester C24H46O7 446 36.478 0.267 171(99), 7(63), 127(45), 99(32), 87(30), 55(21), 73(21), 43(18), 114(17), 172(14) 0.267
28. E-9-Methyl-8-tridecen-2-ol, acetate C16H30O2 254 36.586 0.037 43(99), 55(57), 97(31), 41(29), 109(17), 69(15), 71(14), 123(12), 112(11),57(11) 0.037
29. Cyclohexanol, 2-methyl-3-(1-methylethenyl)-, acetate, (1α,2α,3α)- C12H20O2 196 38.058 0.065 43(99), 136(24), 93(18), 121(18), 41(17), 55(13), 107(12), 95(12), 81(12), 94(10) 0.065
30. Tert-Hexadecanethiol C16H34S 258 38.515 0.067 57(99), 69(76), 43(71), 71(68), 55(61), 83(57), 41(54), 85(47), 97(35), 70(28) 0.067
31. Methyl-2-methoxyoct-2-enoate C10H18O3 186 39.112 0.082 43(99),41(47), 115(44), 55(38), 85(36), 45(34), 69(27), 109(25), 29(24), 42(21) 0.082
32. 7-(1-Hydroxy-cyclohexyl)-2,2-dimethyl-hept-5-en-3-one C15H26O2 238 41.82 0.202 57(99), 85(44), 99(40), 81(35), 41(26), 55(21), 29(17), 83(14), 86(11), 43(10) 0.202
33. Tetradecanoic acid C14H28O2 228 43.242 0.046 73(99), 60(84), 43(68), 57(60), 41(46), 55(45), 129(37), 71(33), 69(28), 85(24) 0.046
34. Phen-1,4-diol, 2,3-dimethyl-5-trifluoromethyl- C9H9F3O2 206 43.987 0.105 149(99),83(29),43(27),151(26),57(24), 55(23), 69(16), 71(15), 77(14), 41(13) 0.105
35. Estra-1,3,5(10)-trien-17β-ol C18H24O 256 44.366 0.071 43(99), 57(99), 55(71), 41(55), 73(47), 71(44), 45(39), 85(35), 83(35), 256(34) 0.071
36. 2-Pentadecanone, 6,10,14-trimethyl- C18H36O 268 44.936 0.077 43(99), 58(89), 71(45), 57(42), 59(40), 41(37), 55(34), 69(24), 85(22), 95(20) 0.077
37. Pentadecanoic acid C15H30O2 242 45.054 0.061 73(99), 60(87), 43(86), 57(81), 41(73), 55(64), 71(49), 129(45), 69(40), 29(36) 0.061
38. Pentadecanoic acid C15H30O2 242 45.987 0.091 73(99), 60(87), 43(86), 57(81), 41(73), 55(64), 71(49), 129(45), 69(40), 29(36) 0.091
39. 1-Hexadecanol, 2-methyl- C17H36O 256 46.126 0.073 57(99), 43(88), 55(67), 41(63), 69(58), 56(57), 71(51), 83(46), 97(38), 70(34) 0.073
40. 2-Butenal, 2-methyl-4-(2,6,6-trimethyl-1-cyclohexen-1-yl)- C14H22O 206 46.683 0.077 107(99), 123(96), 41(72), 206(72), 95(70), 81(64), 55(64), 191(63), 121(59), 135(59) 0.077
41. Z-(13,14-Epoxy)tetradec-11-en-1-ol acetate C16H28O3 268 47.671 0.077 43(99), 97(48), 69(48), 55(44), 41(36), 82(30), 67(29), 81(29), 84(27), 83(27) 0.077
42. n-Hexadecanoic acid C16H32O2 256 53.368 0.496 60(99),73(98), 57(84), 43(81), 55(76), 41(57), 129(43), 71(37), 69(35), 83(26) 0.496
43. cis-13-Octadecenoic acid C18H34O2 282 62.93 0.436 55(99), 69(54), 41(46), 83(43), 97(39), 84(24), 43(24), 56(24), 67(22), 96(21) 0.436
44. 6-Octadecenoic acid C18H34O2 282 63.897 0.244 55(99), 97(85), 83(82), 69(75), 84(64), 96(62), 81(61), 57(54), 264(49), 67(48) 0.244
45. 7-Methyl-Z-tetradecen-1-ol acetate C17H32O2 268 69.535 0.076 43(99), 55(66), 41(50), 81(26), 57(24), 85(23), 67(22), 69(22), 99(21), 83(20) 0.076
46. Z-5-Methyl-6-heneicosen-11-one C22H42O 322 70.771 0.085 43(99), 55(87), 57(81), 41(75), 71(57), 83(47), 169(44), 85(43), 81(40), 69(40) 0.085
47. Hexadecanoic acid, 3-[(trimethylsilyl) oxy]propyl ester C22H46O3Si 386 72.529 0.058 57(99), 43(86), 239(76), 73(68), 71(60), 130(52), 55(50), 41(48), 75(46), 85(38) 0.058
48. Heptacosane C27H56 380 72.942 0.051 57(99), 43(79), 71(62), 85(41), 55(28), 41(27), 69(17), 99(14), 56(13), 29(13) 0.051
49. 1,2-Benzenedicarboxylic acid, diisooctyl ester C24H38O4 390 73.918 0.06 149(99), 167(35), 57(34), 70(26), 41(22), 71(22), 55(21), 43(20), 150(10), 83(10) 0.06
50. Di-n-octyl phthalate C24H38O4 390 74.505 0.05 149(99), 167(54), 57(44), 71(35), 70(28), 43(27), 279(21), 41(21), 113(20), 55(16) 0.05
51. 1,3,2-Dioxaborolane, 4,4′-(1,4-butanediyl)bis[2-ethyl- C12H24B2O4 254 79.581 0.049 99(99), 98(32), 43(27), 41(17), 57(17), 83(13), 138(12), 29(11), 42(10), 55(10) 0.049